1. Introduction
In general, sheet-type waterproofing materials are commonly applied to the vertical surfaces of concrete structures. To ensure the continuous performance of sheet-type waterproofing materials, it is crucial to maintain the long-term adhesion between the substrate and the waterproofing material [
1,
2]. Consequently, many countries have established quality standards for adhesion strength in sheet-type waterproofing materials to manage their performance. The adhesion strength management of sheet waterproofing is typically conducted by physically detaching the sheet material attached to the substrate in a laboratory setting to measure the adhesion strength. However, direct measurement of the adhesion strength for waterproofing layers applied onsite is less prevalent [
3].
As a result, while sheet-type waterproofing materials undergo quality testing by accredited testing agencies to obtain adhesion strength test reports prior to their delivery to the construction site, there are no established test methods or criteria for verifying the adhesion strength after completion of onsite installation. This situation leads to an inability to compare adhesion strength values obtained through laboratory testing with those observed in actual construction settings [
3].
To address the challenges associated with onsite adhesion strength evaluation of self-adhesive waterproofing sheets, researchers and practitioners have conducted various studies on the subject. Several researchers have investigated the effects of environmental conditions on the adhesion performance of self-adhesive waterproofing sheets during onsite installation. For instance, Chenwi et al. explored the impact of prolonged exposure to saline water on the adhesion strength of polyurea [
4]. Previous research by Hedulian et al. explored the general assessment of the adhesion strength indicators of polymer–cement repair materials onto the concrete base and the degree of the repeatability of the results [
5]. Liu et al. provide an extensive study on the topic of the curing process and the thermal failure of the adhesive-bonded structures based on the damping measurement using quantitative electromechanical impedance [
6]. Kim et al. studied the effects of different wet surface conditions on the adhesion strength of the synthetic polymer rubberized gel waterproofing materials and proposed a new method and experimental regime to assess the adhesive performance of the waterproofing material [
7].
In construction sites, sheet waterproofing materials and their adhesion methods can be broadly classified into bond-type adhesion and self-adhesive methods. Bond-type adhesion involves using bonding agents such as asphalt-based or epoxy-based adhesives to attach materials like asphalt sheets, synthetic rubber sheets, and polyvinyl chloride (PVC) sheets to the substrate [
8]. On the other hand, self-adhesive methods involve the factory application of a tacky and flexible rubber asphalt-based adhesive layer to the sheet material, allowing for direct attachment to the substrate without the need for additional adhesives.
Recently, self-adhesive waterproofing sheets have been widely used in the external waterproofing of concrete structures, primarily on vertical surfaces, due to their adhesive flexibility and the convenience of direct attachment without the use of separate adhesives [
9]. This method aims to facilitate the structural response of the system and expedite the installation process.
However, when self-adhesive waterproofing sheets are installed onsite, they are exposed to environmental conditions for a certain period. Prolonged exposure to direct sunlight and temperature fluctuations during the summer season can cause issues such as blistering and delamination of the waterproofing layer, as depicted in
Figure 1 [
10].
To address the issue of deflection in self-adhesive waterproofing sheets, some cases employ a method where structural steel fasteners, as shown in
Figure 2, are used to forcibly restrain and secure the sheets to the structure at the top or intermediate joints of the waterproofing layer [
11].
In the Republic of Korea, for such self-adhesive waterproofing sheets, the adhesion strength is typically measured in the laboratory, according to the attachment strength measurement method specified in KS F 4934 [
12]. However, there is currently no established method to assess the adhesion strength at actual construction sites.
The difficulty in measuring the adhesion strength of sheet waterproofing materials at construction sites stems from the variety of sheet types available (such as asphalt-based, synthetic rubber-based ethylene propylene diene terpolymer (EPDM), and synthetic polymer-based PVC, ethylene-vinyl acetate (EVA), high density polyethylene (HDPE), etc.), as well as the presence of polymer film layers on the sheet surface. Attaching the required equipment for adhesion strength measurement, known as attachments, often necessitates the use of epoxy adhesives without solvents [
9]. However, these epoxy adhesives do not adhere firmly to the polymer film, leading to detachment of the attachments during strength measurements at the adhesive boundary [
13].
Currently, construction practices heavily rely on the skills of workers, lacking appropriate evaluation methods for quality management. Therefore, it is necessary to demonstrate the ability to secure a stable adhesion strength for self-adhesive waterproofing sheets and establish suitable onsite adhesion quality assessment methods to enhance reliability in the waterproofing industry [
13].
This study proposes a new model of an evaluation method that involved developing a field adhesive strength measurement equipment for waterproofing sheets in order to assess the adhesion strength after the installation of self-adhesive waterproofing sheets at a construction site [
14]. A total of six representative types of self-adhesive waterproofing sheets commonly used in domestic construction sites were selected for experimentation. These included two types of rubberized asphalt-based sheets, two types of butyl rubber-based sheets, and two types of adhesive synthetic rubber-based sheets. Hybrid types or modified asphalt waterproofing sheets were excluded to ensure controlled variables.
The experimental methods and conditions were designed to closely resemble real onsite environments. Firstly, deflection resistance tests and shear adhesion strength measurements were conducted on the self-adhesive waterproofing sheets to investigate the causes of deflection. Secondly, an analysis was performed on the phenomena related to delamination through adhesion strength measurements, aiming to understand the underlying principles of adhesion strength manifestation. Lastly, a key focus of this study was to verify whether the onsite adhesion strength measurement equipment aligned with measurements obtained from the laboratory equipment (UTM) for the purpose of introducing the onsite adhesion strength measurement equipment to actual construction sites.
2. Material and Methods
When a liquid droplet exists on a solid surface, the angle formed between the liquid–gas interface and the liquid–solid interface is a measure of how well the solid surface can be wetted by the liquid. When a liquid droplet is present on a solid surface, the balance of two forces determines the shape of the liquid droplet. One force is cohesion, which refers to the attractive forces between the molecules within the liquid itself, and this force tends to make the liquid droplet spherical. The other force is adhesion, which refers to the attractive forces between the liquid and the solid, and this force tends to spread the liquid droplet widely on the solid surface. Therefore, the shape of the liquid droplet is determined by which of these two forces is dominant [
15].
Figure 3 below illustrates this concept.
The contact angle, as shown in
Figure 3, is the angle measured on the inside of the liquid between the liquid–gas interface and the liquid–solid interface. Therefore, when cohesion is dominant, the contact angle increases (close to a sphere), and when adhesion is dominant, the contact angle decreases (spreads widely). When a liquid exhibits a small contact angle and spreads completely on the solid surface, it is referred to as hydrophilic, and significant wetting occurs. The solid surface is said to be hydrophilic. On the other hand, when the liquid exhibits a large contact angle, with minimal wetting occurring on the solid surface, and water droplets roll on the surface, it is referred to as super-hydrophobic. In this case, the liquid exists as separate nearly spherical liquid droplets on the solid surface [
15]. Based on these principles, for adhesive strength measurement, it is important to clearly outline the key parameters to develop a quantitative measurement method with minimal influence from the fewest variables possible. For this, reference to existing adhesion strength measurement methods and outlining the key principles of these methods is required.
2.1. Types of Adhesion Strength Measurement Methods for Self-Adhesive Waterproofing Sheets (Laboratory Testing Methods)
For adhesion peel testing, various methods exist, including the roller drum peel method and 90° and 180° peel adhesion testing. These methods, as shown in
Figure 4, are employed to measure the adhesion strength. While there may be slight variations in certain test conditions, such as the sample size and testing speed, the testing methods remain consistent across both domestic and international standards [
16,
17].
However, all existing adhesion strength testing methods, including those shown in
Figure 4, require the use of an UTM or specialized peel testing equipment, where the force is applied vertically. Currently, there are no specific testing standards available to measure the adhesion strength of waterproofing sheets adhered to vertical concrete surfaces.
The only relevant adhesion strength testing standard for waterproofing sheets is the peel-out test specified in KS F 4934, which does not allow for testing on vertical surfaces. The roller drum peel method shown in
Figure 4a, the American Society for Testing and Materials (ASTM D 3167) [
18], is the most similar to the peel-out test method in KS F 4934 and can be considered a Korean adaptation of that method. In this method, when the waterproofing sheet is pulled by the crosshead, the substrate moves in proportion to the distance the sheet is peeled.
The 180° peel method shown in
Figure 4b [
19] requires the sample to be peeled off the concrete surface while maintaining a 180° angle. This makes it difficult to secure the sample to the testing equipment. Even if the sample is attached, when measuring in the vertical or horizontal directions, the uneven concrete surface can affect the applied load on the measurement area due to the movement of the crosshead. Additionally, due to Newton’s third law of motion (action–reaction principle), if the ends of the waterproofing sheet are not securely fixed, there is a risk of the testing equipment hanging on the sheet when the crosshead pulls a portion of the sheet with greater adhesion strength than the load of the testing equipment. This can lead to measurement errors. Furthermore, the results obtained may differ from the quality inspection results specified in KS F 4934.
The 90° peel method shown in
Figure 4c, is the method outlined in ASTM D6862-11 [
20], where the tested specimen is affixed to the grips of the testing machine with the adhesive bond area exposed. The test is performed at a specified peel angle (90° degrees) and at a constant crosshead speed (commonly 300 mm/min). The testing machine pulls the adherends apart until the adhesive bond fails and records the maximum force required for peeling. It is important that the crosshead moves upward while the sliding plate connected to the wire beneath the specimen maintains the same movement speed as the crosshead. However, to measure a sample adhered to a concrete substrate, both the main body of the testing equipment and the crosshead need to move simultaneously and consistently.
2.2. Peel-Out Test Method and Calculation of Measurement Results
The calculation method for the peel-out test measurement results, as specified in KS F 4934, is described in
Figure 5. The test specimen is passed through a sliding jig, and one end that is not adhered to the test substrate is fixed to the tension testing device, ensuring a peel angle of 90 ± 5°. The sheet is then peeled by 20 mm, excluding the initial peel length, and gradually pulled at a tensile speed of 100 mm/min.
For the peel-out test, the load–peel length curve is divided into four equal sections beyond the initial peel length of 20 mm, as shown in Equation (1). The peel load values (P1, P2, P3, P4, and P5) at the intersection points (
) of the division lines and the load curve are read as the measurement values of the test specimen. The result is based on the average value that is calculated from measurements taken on five specimens [
4].
where
F = Adhesive Strength (N/mm);
Pi = Force (N).
2.3. Development of Onsite Adhesion Strength Measurement Equipment
When measuring the adhesion strength of waterproofing sheets adhered to concrete surfaces in the field, it is necessary to measure the force of the sheet peeling vertically from the concrete substrate. However, applying the roller drum peel method can be challenging due to the inability to move the substrate when measuring the adhesion strength of the waterproofing sheets attached to actual concrete walls or floors.
Among the existing methods, the 90° peel method ensures that the peel length of the sample and the distance traveled by the crosshead are equal. By drawing a graph depicting the relationship between the crosshead’s movement and the distance between the test specimen’s backing cellulose fiber reinforced cement (CRC) board as shown in
Figure 6, it is observed that the graph precisely follows a 1:1 ratio at a 45° angle. Based on this observation, the testing equipment was designed assuming the movement of the crosshead at a 45° angle while peeling the sample. The graph represents a theoretical measurement process during a peel-off of a waterproofing sheet, where the relevant data of the linear regression line for the crosshead displacement relative to the displacement occurring on the CRC board (blue line, marked by blue circles for the intersection points (
) for Equation (1)) is demarcated by the red area.
Therefore, the adopted approach for direct onsite measurements is based on the 90° peel method or a modified roller drum peel method as the foundation. To propose and develop the onsite adhesion strength measurement equipment, several important factors were considered. Firstly, the movement of the equipment during measurements should not transfer its weight onto the sample. Secondly, lightweight design was prioritized to ensure mobility for onsite measurements. Thirdly, the equipment should allow for immediate confirmation of measurement results at the site. Lastly, the ability to measure the adhesion strength of self-adhesive waterproofing sheets applied to vertical surfaces was a key focus. Taking these considerations into account, a design was created as shown in
Figure 7, and a physical prototype was produced as depicted in
Figure 8.
Some important factors that influence the adhesive peel strength include the specimen thickness, the measurement speed, and the onsite temperature. Among these factors, a higher measurement speed results in a higher adhesive peel strength measurement. In the case of KS F 4934, the specified measurement speed was 100 mm/min, which corresponds to the vertical movement speed of the tension jig. However, for the developed onsite equipment, considering that the tension jig moved at a 45° angle, the distance traveled by the tension jig differed by √2 due to the trigonometric calculations. To align the measurement speed with the UTM, it was set to 141 mm/min. Preliminary measurement results showed very similar values to the adhesive peel strength measured by the UTM for the same sample. Based on these results, further testing was conducted.
4. Conclusions
To establish quantitative quality control standards for self-adhesive waterproofing sheets used in construction, it is essential to develop onsite inspection equipment with evaluation capabilities equivalent to laboratory equipment. While construction standards such as KS F 9001, KS F 9003, and KS F 9006 have been established, there is a lack of quantitative inspection methods and criteria for the post-construction assessment of self-adhesive waterproofing sheets, relying solely on the skills of the installers.
Therefore, in this study, to establish a standardized testing method for measuring the adhesive strength of onsite installed self-adhesive waterproofing sheets, a comparison was made between the laboratory measurement method and the onsite measurement method, including the test results and quality criteria. The following conclusions were drawn:
During the peel-out test, it was observed that discrepancies occurred between the test substrate and the test sample. When the adhesive strength of the adhesive layer was higher than the tensile strength of the upper polymer film, differences in elongation occurred between the adhesive area and the self-adhesive waterproofing sheet due to the elongation of the polymer film. Additionally, deviation from the 90° angle between the test substrate and the tensile jig was observed. To control these variables, fabric tape was used to reinforce and restrict the elongation of the polymer film, allowing for the measurement of the pure adhesive peel-out force.
Among the factors affecting the peel-out force, such as the sample thickness, the testing speed, and the onsite temperature, the testing speed showed a significant impact. Higher testing speeds resulted in a higher peel-out strength. To account for the difference in the displacement due to the movement of the tensile jig at a 45° angle in the onsite equipment compared to the vertical movement in the UTM, a testing speed of 141 mm/min was selected for the onsite measurements to match the UTM speed. As a result, the peel-out strength measurements from the onsite equipment closely matched those obtained from the UTM for the same samples. However, the results presented in this study should not yet be taken to state that the method is empirical. There are multiple factors that will need to be taken into consideration, and surely modifications to the equipment are mandatory. The purpose of this article is to simply provide the information that such a method called “onsite/in-situ field equipment for measuring adhesive strength of installed waterproofing method” is important and is in development. Also, the results of repeated testing have shown that the equipment is capable of reproducing results that otherwise would have been yielded using a UTM machine at a reliable rate. However, in-situ installed waterproofing materials are not conveniently placed all the time such that a clean and reliable specimen can be acquired at any moment and place. These specimens could be exposed in areas dangerous to reach for researchers, areas where the equipment may not fit, may not be able to secure the correct angle, submerged, etc. These factors will need to be identified and addressed with further studies.
It is crucial to consider the behavior of the polymer adhesive layer, which relies on time-dependent properties, during the material production process. Enhancements should be made to ensure long-term waterproofing performance, resistance to sagging, and long-term adhesion strength by improving the resistance to viscoelastic deformation of the polymer adhesive layer. Solutions for these challenges are already known in the industry but require collective efforts from stakeholders and organizations for practical implementation.
This study focused on selected representative samples from each category, totaling six types, and may not fully represent all the self-adhesive waterproofing sheets used in the domestic market. Therefore, further research is needed to validate and supplement the findings of this study using a larger sample size.